旋轉電極
RxE 10kTM旋轉電極(產品號:992-00146)是一種研究級旋轉器,它與旋轉環盤和圓柱形電極都適配,可在電化學電池中充當工作電極,使用任何Gamry電化學工作站進行測量。
RxE 透過數位(USB)或類比控制。 轉速為50-10500 rpm,精度為 +/-1 rpm。 一體式軸設計可在高轉速範圍內旋轉。
裝置包含:
- 旋轉器
- 帶可調高度支架的底板
- 電機控制單元和控制電纜
- 電源
- USB 電纜
- 不包括旋轉桿
概述
RxE 10k旋轉電極是一種研究級旋轉器,它與旋轉環盤、圓盤和圓柱形電極都適配。 其轉速調節範圍廣泛,從50 ~10050 rpm(每分鐘轉數),適合不同實驗的需求。 控制器配備液晶顯示幕 ( LCD ),直觀顯示當前轉速,可通過轉速旋鈕控制。 此外,Gamry軟體介面或Reference系列儀器可以實現更精細的轉速控制。 旋轉器電極元件具有通用性,支援多種電極類型。 可以根據實驗需求,靈活選擇不同的旋轉桿和電極頭來進行圓盤和圓柱體或環盤實驗。
應用
腐蝕
催化劑開發
燃料電池研究
控制反應物向電極表面的物質傳輸
旋轉圓環-圓盤電極(RRDE)用於在圓盤電極處監測生成物。 此類實驗需要配備雙恆電位儀。 Gamry提供一台專用儀器,使用兩台Gamry標準恒電位儀連接至同一電腦,實現數據同步收集。 此外,還提供多種RRDE配置,包括鉑-鉑電極、金-金電極以及玻碳-玻碳電極,滿足多樣化的實驗需求。
旋轉盤實驗的實驗條件:確定樣品電極的反應物與生成物品質傳輸,催化劑評估等。
旋轉圓柱實驗對於石油產業至關重要,它可以類比管道內的腐蝕環境,從而省去了流量迴路裝置的高昂開支。 旋轉器是一種理想的工具,即使在低轉速下,轉輪處通常也能維持紊流的流動狀態。 圓筒可採用多種不同金屬製成材料,包括1018碳鋼、316不鏽鋼和430不鏽鋼,以評估其腐蝕性能。 同時,還支援使用者根據實際材料定製加工圓筒樣品。
旋轉器的電極需單獨購買,覆蓋廣泛的標準物質材料,如金、鉑、玻碳、碳鋼、不鏽鋼等。 此外,我們還提供材料定製服務。
規格 |
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功率 |
100 - 240 VAC, +/-10%; 50/60 Hz; 2A |
裝運資訊 |
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裝運重量 |
60 pounds (25 kg) |
通航尺寸 |
24.0 x 20.0 x 24.0 in (61 x 51 x 61 cm) |
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尺寸(長*寬*高) |
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控制裝置 |
11.4 x 10.1 x 5.75 in (29 x 26 x 15 cm) |
旋轉外殼 |
18.8 x 15.5 x 21.0 in (48 x 40 x 54 cm) |
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馬達 |
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馬達功率 |
147 W rated power |
電源電壓 |
48 VDC |
馬達 |
無刷直流馬達 (BLDC) |
馬達保護 |
2 A 熱式斷路器限流電源 |
最大連續轉矩 |
30 millinewton-meters |
轉速控制 |
安裝在馬達軸上的閉環伺服系統溫度補償轉速計 |
轉速顯示 |
4 ½ 位數顯示器指示轉速 (RPM) |
轉速精度 |
+/- 1 rpm for 50-10500 rpm |
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控制 |
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面板 |
類比和數位控制 |
其他 |
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類比和數位控制基板和安裝電極頭之間的最大距離 |
263 cm (RDE); 258 cm (RCE); 261 cm (RRDE) |
The RxE 10kTM Rotating Electrode (Part #992-00146) is a research-grade rotator and features the ability to use rotating ring-disk and cylinder electrodes. It can be used as the working electrode in any electrochemical cell with any Gamry potentiostat.
The RxE is digital (USB) or analog controlled. Rotation rates are 50-10500 rpm. Our one-piece shaft design actually allows us to rotate at those speeds. The RxE accuracy over this rotation rate range is +/- 1rpm.
- Includes:
• Rotator
• Baseplate with adjustable height stand
• Motor Control Unit and control cable
• Power Supply
• USB Cable
Does not include shaft
Overview
The RxE 10k Rotating Electrode is a research-grade rotator and features the ability to use rotating ring-disk, disk and, cylinder electrodes. The rotation rate is adjustable from 50 – 10500 rpm (revolutions per minute). The Controller has a Liquid Crystal Display (LCD) which indicates the rotation rate and is controlled by a rotation rate knob. Alternatively, the rotation rate may be controlled by your Gamry Interface or Reference family instrument. The electrode assembly of the rotator has a versatile design that allows for the use of diverse electrode types. Different shaft and electrode tips can be selected depending on your desired use. Different shafts are used for disk and cylinder or ring–disk experiments.
Applications
- Corrosion
- Catalyst Development
- Fuel Cell Research
- Controlling Mass Transport of Reactants to Electrode Surface
Rotating ring-disk electrodes are used where products generated at the disk electrode are monitored at the ring electrode. A bipotentiostat is required for these experiments and Gamry can supply an instrument using two standard Gamry Potentiostats collecting data synchronously when connected to the same computer. A number of ring-disk electrodes are available including platinum-platinum, gold-gold and glassy carbon-glassy carbon.
Rotating disk experiments are performed where defined mass transport to the sample electrode is desired. An example of this type of experiment would be catalyst evaluation.
Rotating cylinder experiments are important in the oil industry to simulate the corrosion environment inside a pipeline, thus avoiding the need to assemble expensive flow loop setups. The rotator is an ideal tool because flow conditions at the rotating cylinder are generally turbulent even at low rotation rates. Cylinders can be made from a variety of different metals to evaluate their performance including 1018 carbon steel, 316 stainless steel and 430 stainless steel. Users can machine cylinder samples using their actual material.
The electrodes for the rotator are sold separately and include a wide selection of standard materials such as gold, platinum, glassy carbon, carbon steel, stainless steel, etc. Custom materials are available on request.
Specifications
SPECIFICATIONS |
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Power | 100 - 240 VAC, +/-10%; 50/60 Hz; 2A |
SHIPPING INFORMATION |
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Shipping Weight | 60 pounds (25 kg) |
Shipping Dimensions | 24.0 x 20.0 x 24.0 in (61 x 51 x 61 cm) |
DIMENSIONS
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Control Unit | 11.4 x 10.1 x 5.75 in (29 x 26 x 15 cm) |
Rotator Enclosure: | 18.8 x 15.5 x 21.0 in (48 x 40 x 54 cm) |
MOTOR |
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Motor Power | 147 W rated power |
Supply Voltage | 48 VDC |
Motor Type | Brushless DC (BLDC) motor |
Motor Protection | 2 Amp thermal-type circuit breaker current limited power supplies |
Max. Continuous Torque | 30 millinewton-meters |
Rate Control | closed loop servo-system temperature compensated tachometer mounted on motor shaft |
Rate Display | 4 ½ digit display indicates rotation rate (RPM) |
Rate Accuracy | +/- 1 rpm for 50-10500 rpm |
CONTROLS |
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Front Panel | Analog and Digital Control |
MISC. |
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Max distance between baseplate and mounted electrode tip | 263 cm (RDE); 258 cm (RCE); 261 cm (RRDE) |